Figure 3: 1H NMR and NOE spectra of octahedron 1.
From: Assembled molecular face-rotating polyhedra to transfer chirality from two to three dimensions
1H NMR spectrum was measured in dichloromethane and fully rationalised by matching the crystal structure and 2D NMR spectra. The inserted NOE spectrum exhibits the crosspeaks of Hd–Hb and Hd–He1, suggesting Hd is spatially close to Hb and He1 in solution, as presented in the molecular structure (only one butyl chain is shown for clarity).
