Table 1 Data collection and refinement statistics.

From: Linear ubiquitination is involved in the pathogenesis of optineurin-associated amyotrophic lateral sclerosis

 

OPTN/tetraubiquitin

Data collection

 Space group

P212121

 Cell dimensions

 

a, b, c (Å)

71.3, 82.0, 244.9

α, β, γ (°)

90.0, 90.0, 90.0

 Resolution (Å)

50–2.69 (2.86–2.69)*

 Rmerge (%)

14.1 (92.0)

 I/σ I

12.6 (2.24)

 CC1/2 (%)

99.7 (70.4)

 Completeness (%)

99.4 (96.3)

 Redundancy

7.3 (7.3)

Refinement

 Resolution (Å)

49.06–2.69

 No. reflections

40,445

 Rwork/Rfree (%)

20.1/25.4

 No. atoms

 

Protein

6643

Water

59

 B-factors (Å2)

 

Protein

63.08

Water

37.27

 Root mean square deviations

 

Bond lengths (Å)

1.13

Bond angles (°)

0.010

  1. OPTN, optineurin.
  2. *Highest-resolution shell is shown in parenthesis. X-ray data were collected from a single crystal.
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