Table 1 Data collection and refinement statistics.

From: Structural and functional characterization of a calcium-activated cation channel from Tsukamurella paurometabola

 

Dataset 1 (5CBF)

Dataset 2 (5CBG)

Dataset 3 (5CBH)

Data collection

 Space group

I4

I4

I4

 Cell dimensions

a, b, c (Å)

116.05, 116.05, 132.58

115.57, 115.57, 127.49

116.47, 116.47, 128.13

α, β, γ (°)

90, 90, 90

90, 90, 90

90, 90, 90

 Resolution (Å)

50–3.60 (3.66–3.60)*

50–3.15 (3.20–3.15)*

50–3.37 (3.42–3.37)*

 Rsym or Rmerge 14.4 (75)

16 (66.5)

20.9 (86.7)

 

 I/σI

3 (2.85)

3.11 (3)

3 (2.42)

 Completeness (%)

99.3 (99.6)

98.7 (92.2)

96.2 (98.3)

 Redundancy

4.8 (4.5)

4.9 (4.4)

3 (3.1)

Refinement

 Resolution (Å)

50–3.6

50–3.15

50–3.37

 No. reflections

9,567

11,407

13,791

 Rwork/Rfree

23.87 (27.9)

23.68 (29.8)

23.22 (26.2)

 No. atoms

4,627

4,771

4,633

Protein

4,620

4,620

4,620

Detergent/Ca2+

0/3

99/8

0/8

Water

—

36

1

 B-factors

Protein

114.5

65.5

88

Detergent/ Ca2+

0/125

46.7/83.8

0/75.9

Water

—

38.4

8.83

 R.m.s. deviations

Bond lengths (Å)

0.015

0.013

0.014

Bond angles (°)

2.23

1.88

1.95

  1. R.m.s., root-mean-square.
  2. *Values in parentheses are for highest-resolution shell.
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