Table 1 Nm ΔN-PilE data collection and refinement statistics.
Data collection | Nm ΔN-PilE |
|---|---|
Beamline | SSRL 7-1 |
Wavelength (Å) | 0.9753 |
Space group | P212121 |
Cell a, b, c (Å) | 43. 5, 46.3, 48.4 |
Cell α, β, γ (°) | 90.0, 90.0, 90.0 |
Resolution (Å) | 1.44 |
Completeness (%) | 98.7 (88.1)* |
No. of observed reflections | 118934 |
No. of unique reflections | 18088 |
Rmeas (%) | 6 .0 (60.7) |
R-factorobs | 5.5 (53.9) |
I/σ(I) | 21.6 (2.8) |
Wilson B value (Å2) | 18.7 |
Mosaicity (°) | 0.5 |
Refinement | |
Resolution limits (Å) | 33.43-1.44 |
Z | 4 |
No. of reflections used | 18030 |
Rcryst (%) | 18.7 |
Rfree (%) | 21.0 |
No. of non-hydrogen atoms: | |
Protein | 1037 |
Water | 156 |
Avg B factor (Å2): | |
Protein | 16.5 |
Water oxygen | 24.8 |
RMSD bond lengths (Å) | 0.004 |
RMSD bond angles (°) | 0.679 |
Ramachandron plot | |
Favoured (%) | 94.2 |
Allowed (%) | 5.8 |
Outlier (%) | 0 |
PDB ID | 5JW8 |
