Table 1 Data collection, phasing and refinement statistics.
From: Structural and functional analysis of the human POT1-TPP1 telomeric complex
Native (Zn data) | Phasing Hg derivative 1 | |
|---|---|---|
Data collection | ||
Wavelength (Å) | 1.0332 | 1.0000 |
Space group | P4122 | P4122 |
Cell dimensions | ||
a, b, c (Å) | 99.5 99.5 122.1 | 99.0 99.0 124.2 |
Resolution (Å) | 38.6−2.1 (2.15−2.1)* | 40–3.00 (3.08–3.00) |
I/sI | 22.8 (2.7) | 12.3 (3.5) |
Completeness (%) | 99.8 (100) | 99.9 (100) |
Redundancy | 31.3 (31.4) | 7.6 (7.6) |
Phasing analysis | ||
Resolution (Å) | 40−3.00 | |
Number of sites | 5 | |
Pseudo-free CC: | 68.2 | |
Mean figure of merit (FOM) | 0.605 | |
Refinement | ||
Resolution (Å) | 20-2.1 (2.16−2.10) | |
No. reflections | 34,593 (2,473) | |
Rwork/ Rfree | 18/22 (20.8/25.5) | |
No. atoms | ||
Protein | 2,858 | |
Water | 531 | |
B-factors | ||
Protein | 40.4 | |
Water | 54.6 | |
R.m.s deviations | ||
Bond lengths (Å) | 0.008 | |
Bond angles (°) | 1.233 | |
Ramachandran plot (%) | ||
Most favoured | 98.9 | |
Allowed | 1.1 | |
