Table 1 Data collection and refinement statistics.

From: Chemically related 4,5-linked aminoglycoside antibiotics drive subunit rotation in opposite directions

Data collection

 

Space group

P212121

Cell dimensions

 a, b, c (Å)

212.10, 435.24, 614.44

 Resolution (Å)*

70–3.1 (3.2–3.1)

 CC1/2*

99.6 (42.5)

 I/σI*

6.53 (0.68)

 Rmeas*

17.8 (106.9)

 Completeness (%)*

86.3 (54.7)

 Redundancy*†

4.9 (1.7)

Refinement

 Resolution (Å)

70–3.0

 Number of reflections

909,645

 Rwork/Rfree

0.2141/0.2816

Number of atoms

 Protein/RNA

291,292

 Ligand/ion

848

 Water

1,729

B-factors

 Protein/RNA

64.3

 Ligand/ion

61.6

 Water

62.3

R.m.s.d.

 Bond lengths (Å)

0.009

 Bond angles (°)

1.29

  1. r.m.s.d., root mean squared deviation.
  2. *Values in parentheses are for the highest-resolution shell.
  3. †Data were measured from 16 crystals.
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