Abstract
A simple ball milling route to the tetrayanoborate anion is presented: The K[B(CN)4] synthesis is one fine example, how a synthesis problem based on solubility may be solved by a ball milling approach. The solid state 13C- and 11B-MAS-NMR spectra have been recorded.
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Pawelke, R. Ball Milling as a Tool Towards Solubility Problems in Synthesis – Simple and Solvent-free Preparation of K[B(CN)4]. Nat Prec (2011). https://doi.org/10.1038/npre.2011.6258.1
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DOI: https://doi.org/10.1038/npre.2011.6258.1
