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Spectral data of 3: 1H NMR (acetone-d6;, 400 MHz, ppm): δ 7.22–6.54 (aromatic), 3.99–3.48 (methylene).; 13C NMR (DMSO-d6;, 100MHz, ppm): δ 157.1–150.5 (aromatic, HO-C), 132.2–119.9 (aromatic), 30.9–29.7 (methylene, o-o), 35.5–34.6 (methylene, o-p).
4: 1H NMR (acetone-d6;, 400 MHz, ppm): δ 3.89–3.48 (methylene, methoxy), 7.13–6.60 (aromatic).; 13C NMR (CDCl3;-d6;, 100 MHz, ppm): δ 157.6–154.4 (aromatic, HO-C), 134.2–109.9 (aromatic), 55.4–54.5 (methoxy), 35.3–34.5 (methylene, o-p).; IR (KBr, cm−1) ν 2996 (aromatic C-H), 2946, 2904 (methylene C-H bond), 2832 (methyl C-H bond).
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Kobayashi, A., Konishi, Gi. Rapid Synthesis of Phenolic Resins by Microwave-Assisted Self-Condensation of Hydroxybenzyl Alcohol Derivatives. Polym J 40, 590–591 (2008). https://doi.org/10.1295/polymj.PJ2008050
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DOI: https://doi.org/10.1295/polymj.PJ2008050
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