Table 1 Crystallographic data collection and refinement statistics

From: Crystal structure of an assembly intermediate of respiratory Complex II

Data collection

 

Beamline

SSRL 9-2

Wavelength

0.97946 Å

Space group

P21

Unit cell

a = 64.6 Å

 

b = 63.3 Å

 

c = 175.6 Å

 

β = 96.9°

Resolution

50–2.6 Å

R sym

0.093 (0.821)

R pim

0.044 (0.395)

I/σ

11.86 (1.2)

Completeness (%)

96.8 (96.4)

Redundancy

5.0 (4.9)

CC1/2

0.908

Refinement

 

Rcryst (%)

19.3

Rfree (%)

25.5

RMS deviation

 

 Bond lengths

0.011 Å

 Bond angles

1.09°

Ramachandran

 

 Favored

86.8%

 Allowed

12%

 Generous

0.9%

 Outliers

0.2%

B-factors FrdA

51 Å2

B-factors SdhE

96 Å2

  1. Values in parentheses are for the highest resolution shell, which contains data from 2.69 to 2.60 Å resolution