Table 1 Data collection and refinement statistics^a,b,c

Data collection

Space group

H32

H32

H32

P4₃2₁2

Cell, Å (a, b, c)

238.9, 238.9, 354.0

239.2, 239.2, 355.3

241.6, 241.6, 344.5

175.1, 175.1, 454.4

Angles (α, β, γ)

90, 90, 120

90, 90, 120

90, 90, 120

90, 90, 90

Wavelength

1.309 Å

1.00 Å

1.00 Å

1.00 Å

Resolution (Å)

49.66–3.80

39.5–4.10

39.8–4.95

39.81–6.78

(3.87–3.80)

(4.32–4.10)

(5.54–4.95)

(7.58–6.78)

R_pim (%)

–

7.4 (84.1)

8.1 (113.7)

14.2 (139.5)

R_merge (%)

53.4 (91.5)

–

–

–

I/σI

4.31 (0.32)

8.2 (1.1)

5.5 (0.8)

5.6 (1.2)

Completeness (%)

99.1 (93.8)

99.8 (99.9)

99.8 (99.9)

99.4 (99.6)

Multiplicity

9.2 (3.2)

11.9 (12.2)

9.9 (9.8)

18.5 (19.3)

CC_1/2

95.9 (35.4)

99.7 (61.3)

99.6 (45.3)

98.7 (64.8)

Refinement statistics

Resolution (Å)

49.66–3.80

39.5–4.10

39.8–4.85

39.81–6.78

(3.87–3.80)

(4.32–4.10)

(5.31–4.85)

(7.58–6.78)

Reflections

  Measured

354394

366818

166902

238633

  Unique

38101

30813

18521

13801

R_work/R_free

24.3/25.7

25.3/26.7

29.4/31.8

37.9/39.1

Wilson B-factor (Ų)

159.8

141.8

261.8

368.3

Number of atoms

  Protein

11,228

11,162

11,151

33,018

  Carbohydrate

842

799

779

264

R.m.s deviations

  Bond lengths (Å)

0.004

0.008

0.011

0.013

  Bond angles  (˚)

0.837

0.945

0.913

1.450