Fig. 6

Hydride region of 1H NMR spectra of RuCl2(PPh3)3 in C6D6/methanol. a RT, argon atmosphere; b RT, H2 atmosphere (1.5 bar), 10 min; c RT, H2 atmosphere (1.5 bar), 2.5 h; d 60 °C, H2 atmosphere (1.5 bar), 30 min; e 60 °C, H2 atmosphere (1.5 bar), 1.5 h