Table 1 Data collection and refinement statistics

From: Structural basis for activation of a diguanylate cyclase required for bacterial predation in Bdellovibrio

 

Full length

FHA:tail

FHA:phosphopeptide

Accession code

6HBZ

6HC0

6HC1

Data collection

Space group

P6522

P212121

P6522

Cell dimensions

a, b, c (Ã…)

176.8, 176.8, 112.1

69.4, 69.4, 129.0

68.8, 68.8, 191

α, β, γ (˚)

90, 90, 120

90, 90, 90

90, 90, 120

Resolution (Ã…)

1.79 (90.45)a

1.87 (36.53)

1.49 (56.84)

R sym

0.120 (>1.0)

0.079 (>1.0)

0.129 (>1.0)

R pim

0.028 (0.455)

0.033 (0.777)

0.030 (0.792)

I/σI

20.4 (2.6)

19.1 (1.4)

16.1 (1.2)

CC ½

0.998 (0.448)

1.0 (0.617)

0.999 (0.545)

Completeness (%)

100 (99.6)

100 (100)

100 (100)

Redundancy

37 (36.9)

12.8 (12.6)

33.5 (24.2)

Refinement

Resolution (Ã…)

1.79

1.87

1.49

No. of reflections

97426

52162

44616

Rwork/Rfree

17.9/21.6

17.7/20.6

14.2/17.8

No. of atoms

Protein

4192

3149

1656

Ligand/ion

113

3

—

Water

439

284

192

B-factors

Protein

35.74

41.95

26.37

Ligand/ion

32.48

37.92

—

Water

44.37

48.01

40.29

R.m.s. deviations

Bond lengths (Ã…)

0.011

0.017

0.016

Bond angles (°)

1.59

1.79

1.70

  1. aValues in parentheses are for highest-resolution shell. Each dataset derives from a single crystal
Back to article page