Table 2 Data collection and refinement statisticsa.
LspMrs-globomycin (6RYO) | LspMrs-myxovirescin (6RYP) | |
|---|---|---|
Data collection | ||
Space group | P3221 | P6122 |
Cell dimensions | ||
a, b, c (Å) | 52.3, 52.3, 135.9 | 54.2, 54.2, 317.5 |
α, β, γ (°) | 90, 90, 120 | 90, 90, 120 |
Beamline | SLS-X06SA | SLS-X06SA |
Wavelength (Å) | 0.92003 | 1.0 |
Resolution (Å) | 45.26–1.92 (2.23–1.92)b | 46.40–2.30 (2.36–2.30) |
No. of reflections (total/unique) | 33,655/7,051 | 199,005/23,038 |
\(R_{\rm{meas}}\) | 0.17 (1.38) | 0.14 (2.79) |
I/σI | 7.00 (1.80) | 7.69 (0.90) |
Completeness (%) | 86.20 (62.50)c | 99.9 (100) |
Multiplicity | 4.80 (3.70) | 8.63 (8.90) |
CC1/2 | 0.99 (0.47) | 0.99 (0.22) |
Refinement | ||
Resolution (Å) | 45.26–1.92 | 46.40–2.30 |
Reflections | 7046 | 23,038 |
\(R_{\rm{work}}/R_{\rm{free}}\) | 0.25/0.28 | 0.25/0.28 |
R.m.s. deviations | ||
Bond lengths (Å) | 0.002 | 0.001 |
Bond angles (°) | 0.498 | 0.372 |
No. of atoms | ||
Protein | 1232 | 1287 |
Globomycin or Myxovirescin | 46 | 44 |
Other ligandsd | 242 | 176 |
Water | 28 | 12 |
B-factor | ||
Protein | 36.78 | 68.15 |
Globomycin or Myxovirescin | 20.87 | 75.61 |
Other ligandsd | 58.91 | 100.05 |
Water | 29.36 | 75.49 |
Ramachandran Plot | ||
Favored (%) | 97.39 | 98.15 |
Allowed (%) | 2.61 | 1.85 |
Outliers (%) | 0 | 0 |
MolProbity Clashscore | 7.87 | 1.32 |
