Fig. 5: Morphology measurements of Ba0.75Sr0.25NiO3 before and after OER testing.

a HRTEM before a stability test. b HRTEM after a stability test. Right side: STEM atomic mapping (scale bar: 500 nm). The labelled lattice spacing is around 0.3 nm, which corresponded to the (110) lattice planes of Ba0.75Sr0.25NiO3, in good agreement with the PXRD measurements. The insets of a, b show the fast Fourier transform image of the corresponding HRTEM image. The well-regulated arrayed spots indicated that the grown crystal had high crystallinity. HRTEM of Ba0.75Sr0.25NiO3 before and after OER testing clearly showed the same lattice spacing and very similar fast Fourier transform images, suggesting outstanding stability of the Ba0.75Sr0.25NiO3 sample under OER conditions. The maintenance of good crystallinity indicates that Ba0.75Sr0.25NiO3 is a stable OER electrocatalyst. In order to verify the atomic distribution, STEM mapping was conducted; the even distribution of the atoms over the analyzed area further demonstrates the excellent stability of the sample.