Table 1 Data processing and refinement statistics for GII.4 P-domain–NORO-320 Fab complex.

Beamline

ALS Beamline 5.0.1

Wavelength, Å

0.97741

Space group

P21 21 2

Cell dimensions, Å

119.25, 186.27, 73.44

α,β,γ,°

90, 90, 90

Resolution, Å

50–2.25 (2.29–2.25)^a

Total reflections

1716311

Unique reflections

78053 (3854)^a

Redundancy

6.5 (6.2)^a

Completeness (%)

99.82

<I/sigma>

15.6875 (2.375)^a

R_meas ^b

0.129 (0.846)^a

R_pim^b

0.050 (0.340)^a

Resolution, Å

50–2.25 (2.29–2.25)^a

Reflections (work)

73965

Reflections (test)

3926

R_work ^c /R_free ^d (%)

18.08/22.55

Protein

P-domain dimer

4798

Noro-320 Fab

6674

Water

1059

P-domain dimer

34.2505

NORO-320 Fab

31.67

Water

36.085

Bond length (Å)

0.003

Bond angle (°)

0.614

Favored

98.38%

Outliers

0.20%