Fig. 2: Morphological evolution of Cu2O cubes and re-deposited NPs captured under operando conditions over 45 min of CO2RR by EC-TEM.

Snapshots extracted from the videos tracking the evolution of a 390 nm, b 170 nm, and c 80 nm cubes at 0, 5, 25, and 45 min after applying a potential of −0.9 VRHE. Each image is an average of 10 frames. The electron flux used is 3.5 e− Å−2 s−1.