Fig. 2: Comparison of NBD and SCED results of a 2D single crystal thin film of α, ω-DH6T bilayer.

a STEM-ADF image of the area of interest (acquired at the end of experiment). Insets show the molecular structure and scheme of the assembled monolayer on the substrate. The white box indicates where 4D-NBD and 4D-SCED data were acquired subsequently. Three representative raw patterns extracted from the positions marked with color dots are shown in b for the NBD results and c SCED results. d intensity profiles of the raw pattern comparing NBD and SCED.