Fig. 2: Development of one-pot operation. | Nature Communications

Fig. 2: Development of one-pot operation.

From: Carbene and photocatalyst-catalyzed decarboxylative radical coupling of carboxylic acids and acyl imidazoles to form ketones

Fig. 2

a One-pot procedure for coupling of two carboxylic acids. b Comparision between one-pot operation and standard conditions. For synthesis of 3b, DMSO was used as solvent; HATU: 2-(7-Azabenzotriazol-1-yl)-N,N,N’,N’-tetramethyluroniumhexafluorophosphate; DCC: N,N’-Dicyclohexylcarbodiimide; DIC: N,N’-Diisopropylcarbodiimide.

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