Fig. 3: Structural characterization data.

a FT-IR spectra and b 13C NMR spectra of TFPA-TAPT-COF-Q (red) and TFPA-TAPT-COF (blue). c XPS spectra of N 1 s in TFPA-TAPT-COF-Q and TFPA-TAPT-COF. d FT-IR spectra and e 13C NMR spectra of TFPA-TPB-COF-Q (orange) and TFPA-TPB-COF (light blue). f XPS spectra of N 1 s in TFPA-TPB-COF-Q and TFPA-TPB-COF. g N2 sorption isotherms of TFPA-TAPT-COF-Q (red) and TFPA-TPB-COF-Q (orange) at 77 K. h Calculated pore size distributions of TFPA-TAPT-COF-Q (red) and TFPA-TPB-COF-Q (orange).