Table 1 Data collection and refinement statistics
GATA18-SAP05 | SPL5-SAP05 | SAP05-RPN10 | SPL13-SAP05 | |
|---|---|---|---|---|
PDB accession number | 8J48 | 8J49 | 8J4A | 8J4B |
Data collection | ||||
Space group | P 21 | P 1 | P 21 | P 21212 |
Cell dimensions | ||||
a, b, c (Å) | 35.84, 73.41, 58.69 | 30.16, 45.09, 52.95 | 54.05, 40.59, 130.33 | 90.92, 63.35, 68.56 |
α, β, γ (°) | 90.00, 107.22, 90.00 | 92.43, 101.86, 108.62 | 90.00, 93.01, 90.00 | 90.00, 90.00, 90.00 |
Resolution (Å) | 36.70-1.94 (2.01-1.94)* | 42.44-1.66 (1.75-1.66) | 48.95-1.97 (2.04-1.97) | 36.93-2.00 (2.07-2.00) |
Rsym or Rmerge | 0.133 (1.006) | 0.034 (0.250) | 0.066 (0.468) | 0.109 (0.627) |
I / σI | 10.79 (1.65) | 11.70 (2.30) | 11.87 (2.85) | 13.74 (3.21) |
Completeness (%) | 97.2 (81.6) | 83.5 (32.5) | 94.6 (98.1) | 99.5 (96.7) |
Redundancy | 6.1 (4.1) | 3.4 (2.9) | 2.8 (2.6) | 9.1 (7.2) |
Refinement | ||||
Resolution (Å) | 36.70-1.94 (2.01-1.94) | 42.44-2.10 (2.18-2.10) | 42.66-1.97 (362.04-1.97) | 34.28-2.00 (2.07-2.00) |
No. reflections | 20846 (1743) | 14114 (1389) | 38214 (3983) | 27304 (2608) |
Rwork / Rfree | 0.1961/0.2371 | 0.1748/0.2113 | 0.1925/0.2526 | 0.1753/0.2132 |
No. atoms | ||||
Protein | 2267 | 2191 | 4596 | 2747 |
Ligand/ion | 2 | 2 | 0 | 4 |
Water | 187 | 180 | 477 | 284 |
B-factors | ||||
Protein | 28.2 | 24.4 | 14.5 | 28.5 |
Ligand/ion | 31.7 | 29.1 | 0 | 38.5 |
Water | 33.4 | 29.7 | 22.0 | 34.9 |
R.m.s. deviations | ||||
Bond lengths (Å) | 0.009 | 0.008 | 0.008 | 0.009 |
Bond angles (°) | 1.01 | 0.96 | 1.12 | 0.94 |
