Fig. 6: Time-dependent decalin encapsulation of 1.
From: Latent porosity of planar tris(phenylisoxazolyl)benzene
a Time-dependent changes in the PXRD pattern for the solvent-free powder with the 1α and 1β phases when exposed to a 1:1 mixture of vaporous cis- and trans-decalin for (A) 0 days, (B) 1 day, (C) 2 days, (D) 5 days, (E) 7 days, and (F) 9 days. The red and blue arrows in Panel b indicate increasing and decreasing trends, respectively. b Plot of normalized PXRD peak intensity of (square) 1α (6.24°), (triangle) 1β (7.62°), and (circle) cis-decalin@1 (7.14°) against time. The bar graph indicates the sum of the normalized intensity, where green, magenta, and blue correspond to 1α, 1β, and cis-decalin@1, respectively.
