Fig. 3: Decarboxylative C(sp³)–C(sp³) cross-coupling reaction scope.

The characterization of the isolated products is described in the Supplementary Material. In gray between brackets, yields reported using homogeneous Ni complex and Ir photocatalyst¹⁸. ^aReaction scaled up to 2 mmol by sizing up. ^bNumbering up strategy of 15 multi-batch reactions.