Fig. 3: Mithrene structure determination results.
From: Chemical crystallography by serial femtosecond X-ray diffraction
a, b, Identification of the C6H5 group in a Fourier difference map. The map is calculated from Fobs − Fcalc coefficients and contours are drawn at intervals of approximately 0.15 e− per Å3. The ring is disordered over two positions; both positions are shown in b, although they nearly overlap in this view. The plots were generated by Olex215. c, d, Crystal structure of mithrene as determined in the present work (c) and the reference single-crystal structure19 (d). e, Plot of candidate unit cells indexing rate versus M* (see equation (1) in Methods). Cell 2, labelled in red, is the correct cell, with the highest indexing rate and a low value of M*.
