Table 1 1H and 13C NMR chemical shifts (ppm) of FVPB2 at 27 °C.
Residue | Proton or carbon | |||||
|---|---|---|---|---|---|---|
H-1/C-1 | H-2/C-2 | H-3/C-3 | H-4/C-4 | H-5/C-5 | H-6/C-6 | |
A α-D-Manp(1 → | 5.17 | 4.12 | 3.91 | 4.06 | 3.82 | 3.56a, 3.70b |
104.02 | 72.73 | 71.48 | 69.48 | 76.19 | 65.21 | |
B - → 3,4)- α-D-Galp(1 → | 5.16 | 3.98 | 4.04 | 4.22 | 3.91 | 3.80a, 3.96b |
105.69 | 73.07 | 80.09 | 77.65 | 71.52 | 63.76 | |
C → 6)-α-D-Glcp(1 → | 5.11 | 3.84 | 3.74 | 3.94 | 4.07 | 3.95a, 3.79b |
100.50 | 76.07 | 73.07 | 72.11 | 72.51 | 69.50 | |
D α-L-Fucp(1 → | 5.09 | 3.89 | 4.12 | 3.91 | 4.23 | 1.28 |
104.10 | 71.52 | 72.73 | 71.52 | 69.91 | 18.36 | |
E → 2)-α-D-Galp-(1 → | 5.06 | 3.90 | 4.07 | 3.93 | 4.27 | 3.68a, 3.94b |
100.59 | 80.26 | 72.23 | 72.15 | 71.52 | 65.24 | |
F → 3,6)-β-D-Glcp-(1 → | 4.58 | 3.38 | 3.56 | 3.69 | 3.91 | 4.26a, 3.92b |
105.58 | 75.76 | 78.30 | 71.35 | 71.52 | 71.52 | |
