Tablet 3 Summary of molecular weight, multiple-reaction monitoring transitions, DP and CE of the 13 components determined by HPLC-MS/MS.
Compound | Molecular weight | Monitoring ion | Precursor ion (m/z) | Product ion (m/z) | DP (V) | CE (eV) |
|---|---|---|---|---|---|---|
AC | 645.7 | ESI+ | 646.3 | 105.1 | 180 | 50 |
MA | 631.7 | ESI+ | 632.2 | 105.1 | 180 | 46 |
HA | 615.7 | ESI+ | 616.3 | 105.0 | 180 | 46 |
BAC | 603.7 | ESI+ | 604.3 | 105.0 | 180 | 45 |
BMA | 589.7 | ESI+ | 590.3 | 105.0 | 205 | 46 |
BHA | 573.3 | ESI+ | 574.3 | 105.0 | 200 | 46 |
Lev | 380.2 | ESI+ | 381.0 | 191.0 | 90 | 10 |
Ino | 268.2 | ESI+ | 268.9 | 136.9 | 80 | 5 |
Lig | 190.2 | ESI+ | 191.0 | 90.9 | 100 | 15 |
Ace | 512.4 | ESI− | 511.3 | 59.1 | 110 | 12 |
Bet | 456.4 | ESI− | 455.3 | 377.4 | 110 | 48 |
Fer | 194.1 | ESI− | 193.0 | 133.8 | 100 | 12 |
Pro | 154.0 | ESI− | 153.0 | 109.0 | 90 | 12 |
