Table 1 Data processing and refinement statistics.

Space group

P 4₃

P 2₁ 2₁ 2₁

a, b, c (Å)

157.96, 157.96, 77.50

119.48, 119.60, 132.99

Resolution (Å)

70.64–2.40 (2.45–2.40)^a

88.93–3.70 (4.05–3.70)^a

No. of unique reflections

74 039 (4 617)^a

20 732 (4 698)^a

Completeness (%)

98.8 (99.9)^a

98.8 (95.3)^a

Multiplicity

6.2 (6.3)^a

6.6 (6.8)^a

Mean ((I)/σ(I))

10.5 (1.9)^a

6.8 (2.8)^a

R_merge (%)

12.3 (147.6)^a

22.4 (69.1)^a

R_pim (%)

4.9 (58.1)^a

9.4 (28.4)^a

CC_1/2

0.996 (0.643)

0.989 (0.819)

R_work/R_free (%)^b

18.13/21.21

24.73/28.82

Bond lengths (Å)

0.003

0.002

Bond angles (°)

0.643

0.510

Coordinate error (Å)

0.32

0.49

Protein^c

9 152

10 230

Carbohydrate

0

155

Solvent

249

0

Other^d

59

0

Favoured (%)

96.59

96.21

Allowed (%)

3.33

3.65