Table 1 Characterisation data for MAPs: reaction yield (%), particle size for flow (CFS) and batch (Bx) produced material as 10th, 50th and 90th percentiles (D10, D50 and D90, µm), BET surface are (m2/g) and observed XRD crystal hydration phase.
From: Low-Temperature Continuous Flow Synthesis of Metal Ammonium Phosphates
M | XRD Phase | Yield | Particle Size (CFS, um) | Particle Size (Bx, um) | Throughput | BET | |||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
(CFS) | (Bx) | % (CFS) | % (Bx) | D10 | D50 | D90 | D10 | D50 | D90 | CFS | Bx | m2/g (CFS) | |
MgAP* | Mon/Hex | Mon | 94 | 99 | 2.5 | 13.6 | 44.3 | 14.6 | 24.6 | 66.0 | 6.6 | 1.3 | 15.7 |
MnAP | Mon | Mon | 99 | 99 | 6.4 | 22.8 | 65.1 | 7.4 | 18.4 | 42.2 | 8.4 | 1.5 | 6.8 |
FeAP | Mon | Mon | 99 | 99 | 2.9 | 9.5 | 23.9 | 15.4 | 52.8 | 108.3 | 8.4 | 1.6 | 49.8 |
CoAP | Mon | Mon | 97 | 99 | 4.9 | 23.5 | 51.3 | 15.8 | 65.0 | 135.9 | 8.4 | 1.6 | 6.5 |
NiAP | Hex | Mon | 83 | 99 | 1.3 | 7.7 | 26.6 | 2.6 | 12.1 | 81.4 | 7.1 | 1.6 | 9.5 |
ZnAP | Anhyd | Anhyd | 98 | 99 | 2.0 | 9.7 | 20.9 | 6.3 | 19.9 | 45.5 | 7.9 | 0.5 | 3.6 |
SnHP | Anhyd | Anhyd | 79 | 78 | 2.7 | 6.5 | 22.8 | 2.3 | 19.4 | 40.3 | 7.5 | 1.5 | 4.7 |
