Table 1 The results of the analysis of the serum examples (200 µL of the serum example with three different concentrations of AA, DA, UA (I, II & III). DPV conditions: 180 s; 0.1 M PBS solution (pH of 3.0); potential range −0.20 to + 0.80 V (UDL: under detection limit).
Serum sample | Found (10−6 M) | Spiked (10−6 M) | Recovery (10−6 M) | % Recovery | ||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|
AA | DA | UA | AA | DA | UA | AA | DA | UA | AA | DA | UA | |
I | UDL | UDL | 33.0 | 100 | 10 | 10 | 96 ± 1.2 | 9.7 ± 0.9 | 42.8 ± 0.3 | 96 | 97 | 99.5 |
II | UDL | UDL | 34.0 | 250 | 25 | 50 | 252 ± 0.4 | 24.6 ± 0.3 | 84.5 ± 0.2 | 100.8 | 98.4 | 100.6 |
III | UDL | UDL | 33.0 | 500 | 50 | 100 | 505 ± 0.3 | 49.9 ± 0.3 | 132.9 ± 0.9 | 101.0 | 99.8 | 99.9 |