Table 1 The data of the main crystallographic characteristics.
T, °C | Cell parameter, Å | Crystalline size, nm | Atomic ratio, Co/O at.w. % | Dislocation density, 1015, 1/m2 | The concentration of vacancy oxygen defects, % | Integral porosity, % | Dendity, g/cm3 |
---|---|---|---|---|---|---|---|
25 | Co-FCC – a = 3.5329; Co-HCP – a = 2.4957, c = 4.0533 | 18.3 ± 2.1 | 100/0 | 2.98 | 0.03 | 0.53 | 8.64 |
100 | Co-FCC – a = 3.5142; Co-HCP – a = 2.4816, c = 4.0653 | 14.6 ± 1.6 | 100/0 | 4.71 | 0.11 | 0.32 | 8.71 |
200 | Co-FCC a = 3.5230; Co-HCP – a = 2.4888, c = 4.0701 | 17.9 ± 1.3 | 95/5 | 3.12 | 0.78 | 0.25 | 8.74 |
300 | Co-FCC a = 3.5292; CoCo2O4 –a = 8.0508 | 16.0 ± 1.5 | 83/17 | 3.91 | 1.82 | 0.78 | 7.43 |
400 | Co-FCC a = 3.5230; CoCo2O4 – a = 8.0301 | 22.6 ± 2.1 | 78/22 | 1.96 | 1.89 | 1.43 | 7.02 |
500 | CoCo2O4 – a = 8.0411 | 31.5 ± 2.5 | 46/54 | 1.01 | 1.98 | 2.34 | 6.07 |
600 | CoCo2O4 – a = 8.0364 | 31.9 ± 2.1 | 43/57 | 0.98 | 2.42 | 2.54 | 6.04 |
700 | CoCo2O4 – a = 8.0396 | 34.9 ± 2.9 | 41/59 | 0.81 | 6.78 | 7.84 | 5.89 |