Table 3 Yields of recovered 5-HMF derived from wood (0.09 g; moisture content 4.8%) by vacuum distillation with [MIM]HSO4 (3 g) at 2.5 kPa.
Reaction temperature (°C) | Reaction time (min) | Yield (wt%) | |
---|---|---|---|
In trap | In [MIM]HSO4 | ||
140 | 240 | 0.1 | 5.6 |
160 | 30 | 0.1 | 6.2 |
180 | 15 | 0.1 | 1.2 |
200 | 15 | 0.3 | 0.5 |