Table 1 Particle (< DTEM >) and crystallite (< DXRD >) average size (nm) obtained from TEM and XRPD analysis, respectively, together with the corresponding calculated volumes.
Sample | < DTEM > (nm) | < DXRD > (nm) | < DTEM > / < DXRD > | VTEM (nm3) | VXRD (nm3) | NC (VTEM / VXRD) |
---|---|---|---|---|---|---|
SFOA | 310 (10) | 132 (11) | \(\cong 2.4\) | 15,598 \(\times\) 103 | 1204 \(\times\) 103 | \(\cong 13\) |
SFOB | 150 (20) | 88 (9) | \(\cong 1.7\) | 1767 \(\times\) 103 | 356 \(\times\) 103 | \(\cong\) 5 |
SFOC | 60 (20) | 63 (6) | \(\cong 1\) | 113 \(\times\) 103 | 130 \(\times\) 103 | \(\cong 1\) |