Table.1 The sample stoichiometry of YbFe2O4.
Raw material rate Fe2O3/Yb2O3 (mol) | Fe/Yb rate (evaluated by XRF) | Stoichiometry of oxygen YbFexOy (evaluated by TGA) | Average of Fe valence |
---|---|---|---|
2.00 | 1.79(3) | x = 1.79, y = 3.775(5) | 2.542(5) |
2.20 | 1.95(3) | x = 1.95, y = 3.960(5) | 2.523(5) |