Table 2 ANOVA for the adjusted variables to the Box-Behnken design: moisture, aw, CA, hab, ΔE*, FDt, contrast, correlation, IDM and entropy for flakes of HOPO nanoemulsions.

From: The effect of process variables on the physical properties and microstructure of HOPO nanoemulsion flakes obtained by refractance window

 

Moisture (%)

aw

CA (°)

hab (°)

∆E*

SS

df

p-value

SS

df

p-value

SS

df

p-value

SS

df

p-value

SS

df

p-value

Model

21.691

19

0.014

0.0602

19

0.0283

44.506

19

0.0287

582.031

19

0.0047

361.620

13

0.8568

A

12.616

1

 < 0.001

0.0264

1

0.0003

16.091

1

0.0007

0.1585

1

0.6504

0.2055

1

0.8408

B

1.096

1

0.099

0.0001

1

0.7707

0.0057

1

0.7991

112.341

1

0.0016

0.6546

1

0.7203

C

0.500

1

0.253

0.0001

1

0.7721

0.0034

1

0.8431

155.746

1

0.0004

94.393

1

0.1831

D

1.190

1

0.087

0.0005

1

0.5353

0.0049

1

0.8141

41.644

1

0.0325

12.809

1

0.6170

AB

0.010

1

0.872

9.59. × 10–7

1

0.9773

0.2546

1

0.1049

0.0181

1

0.8778

0.7426

1

0.7030

AC

0.907

1

0.130

0.0011

1

0.3391

0.0892

1

0.3221

0.6954

1

0.3486

19.124

1

0.5418

AD

0.064

1

0.676

0.0001

1

0.7448

0.2214

1

0.1282

0.3666

1

0.4929

0.6601

1

0.7192

BC

0.578

1

0.221

0.0002

1

0.6778

0.1505

1

0.2038

0.2613

1

0.5617

0.7783

1

0.6963

BD

0.223

1

0.439

0.0005

1

0.5182

0.0122

1

0.7100

0.3028

1

0.5325

141.568

1

0.1068

CD

1.197

1

0.086

0.0001

1

0.7738

0.0001

1

0.9696

23.871

1

0.0940

16.635

1

0.5691

A2

1.172

1

0.089

0.0116

1

0.0066

15.175

1

0.0008

0.1066

1

0.7099

0.8942

1

0.6758

B2

0.009

1

0.874

0.0005

1

0.5044

0.0170

1

0.6610

0.2300

1

0.5859

27.530

1

0.4651

C2

0.086

1

0.628

0.0009

1

0.3915

0.1142

1

0.2649

117.771

1

0.0013

0.5959

1

0.7326

ABD

0.896

1

0.133

0.0083

1

0.0175

0.0226

1

0.6137

0.3240

1

0.5187

–

 

–

ACD

0.346

1

0.338

0.0020

1

0.2031

0.1528

1

0.2006

70.846

1

0.0079

–

 

–

BCD

0.147

1

0.529

0.0004

1

0.5822

0.0566

1

0.4274

0.3270

1

0.5169

–

 

–

A2B

–

–

–

–

–

–

–

–

–

34.180

1

0.0495

–

 

–

A2D

0.003

1

0.931

0.0010

1

0.3568

0.0479

1

0.4645

34.180

1

0.0495

–

 

–

B2D

0.953

1

0.122

0.0016

1

0.2587

0.0021

1

0.8784

0.3133

1

0.5256

–

 

–

C2D

0.570

1

0.223

0.0045

1

0.0672

0.1028

1

0.2892

0.9610

1

0.2734

–

 

–

Lack of fit

3.522

6

0.058

0.0085

6

0.2828

0.3734

6

0.7162

20.427

6

 

495.597

12

0.7475

Pure error

1.396

8

 

0.0075

8

 

0.8123

8

 

83.086

8

 

496.984

8

 

R2

0.815

  

0.7902

  

0.7896

  

0.8490

  

0.2670

  
 

FDt

Contrast

Correlation

IDM

Entropy

SS

df

p-value

SS

df

p-value

SS

Df

p-value

SS

df

p-value

SS

df

p-value

Model

0.0311

13

 < 0.0001

760,691.83

13

 < 0.001

5.77x10–7

13

0.0002

0.0006

13

0.0004

1.0449

13

3.71 × 10–4

A

0.0126

1

 < 0.0001

440,783.29

1

 < 0.001

3.16x10–7

1

 < 0.001

0.0003

1

 < 0.001

0.4446

1

 < 0.001

B

0.0004

1

0.2241

3557.04

1

0.4760

1.14 × 10–9

1

0.6937

2.0 × 10–5

1

0.1413

0.0011

1

0.7870

C

0.0008

1

0.1029

244.67

1

0.8508

7.20 × 10–9

1

0.3278

1.3 × 10–6

1

0.7058

0.0947

1

0.0193

D

2.28 × 10–5

1

0.7786

416.98

1

0.8061

4.08 × 10–11

1

0.9406

1.5 × 10–6

1

0.6766

0.0001

1

0.9236

AB

4.03 × 10–6

1

0.9059

126.59

1

0.8924

1.13 × 10–9

1

0.6952

7.0 × 10–6

1

0.3775

7. × 10–6

1

0.9827

AC

0.0003

1

0.3045

28,624.14

1

0.0526

4.17 × 10–9

1

0.4543

3.2 × 10–5

1

0.0685

0.0154

1

0.3172

AD

1.52 × 10–5

1

0.8184

318.22

1

0.8302

2.19 × 10–10

1

0.8629

1.1 × 10–5

1

0.2817

0.0068

1

0.5037

BC

4.78 × 10–5

1

0.6845

933.75

1

0.7137

4.26 × 10–10

1

0.8097

2.5 × 10–6

1

0.5941

0.0016

1

0.7457

BD

0.0006

1

0.1543

301.61

1

0.8346

1.02 × 10–8

1

0.2474

1.4 × 10–5

1

0.2164

0.0304

1

0.1652

CD

0.0002

1

0.4586

500.51

1

0.7881

1.20 × 10–9

1

0.6867

6.2 × 10–8

1

0.9330

0.0301

1

0.1669

A2

0.0138

1

 < 0.0001

273,923.46

1

0.0000

2.35 × 10–7

1

 < 0.0001

0.0002

1

 < 0.0001

0.3929

1

 < 0.0001

B2

2.1 × 10–5

1

0.7890

1598.71

1

0.6316

6.46 × 10–13

1

0.9925

1.3 × 10–6

1

0.6969

0.0173

1

0.2892

C2

0.0028

1

0.0048

12,319.32

1

0.1915

9.15 × 10–10

1

0.7244

9.6 × 10–7

1

0.7423

0.0016

1

0.7417

ABD

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

ACD

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

BCD

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

A2B

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

A2D

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

B2D

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

C2D

–

–

–

–

–

–

–

–

–

–

–

–

–

–

–

Lack of fit

0.0020

12

0.9433

43,465.57

12

0.9639

2.63 × 10–8

12

0.9981

0.0001

12

0.9769

0.1401

12

0.7864

Pure error

0.0036

8

 

91,366.54

8

 

1.17 × 10–7

8

 

0.0001

8

 

0.1526

8

 

R2

0.8468

  

0.849

  

0.8011

  

0.7776

  

0.7812

  
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