Table 1 Summary of hot particle characterization results using µ-SXRF, µ-XAS, and µ-XRD techniques.

From: The nature of Pu-bearing particles from the Maralinga nuclear testing site, Australia

Particle name

Locality

Description

Major elemental composition

Oxidation state of Pu, U present

Major mineral composition

Bruce (GNE*)

North-east plume

Irregular, uneven oblong particle with bumpy surface. Length = 518 µm

Pu, U, Fe, Al

Pu(0) + Pu(IV) ± Pu(III), U(IV/VI)

Pu–U-C, PuO2±x, UO2±x/U3O7, Al–Fe alloy/Al2O3

Potatohead (ZD600*)

North-west plume

Irregular trapezoidal shape with uneven surface. Length = 336 µm

Pu, U, Al, Fe

Pu(IV), U(IV/VI)

PuO2±x, UO2±x/U3O7

CeresI (K480i)

100 m north GZ

Spherical, slightly oval particle with smooth surface containing slight imperfections. Length = 218 µm

Pb, Pu, U

Pu(IV), U(IV)

Native lead

CeresII (K480iI)

100 m north GZ

Irregular, somewhat spherical particle with square protrusion on surface. Length = 216 µm

Pb, Pu, U

n/a

Native lead

CeresIII (K480iii)

100 m north GZ

Spherical particle with smooth surface containing slight imperfections. Length = 222 µm

Pb, Pu, U

n/a

Native lead

Chip (K480iv)

100 m north GZ

Irregular, oblong particle with smooth surface. Length = 110 µm

Pb, Pu, U

n/a

Native lead

  1. *Particles from study of Burns and co-workers5,7.