Table 5 Precision data for the assay of FAV and APX in their raw materials.
FAV | APX | ||||
|---|---|---|---|---|---|
Sample concentration (ng mL−1) | % Recoverya (Intraday precision) | % Recovery* (inter-day precision) | Sample concentration (μg mL−1) | % Recovery* (Intraday precision) | % Recovery* (inter-day precision) |
4 | 99.52 | 99.14 | 0.4 | 100.03 | 98.28 |
98.37 | 97.91 | 100.65 | 99.85 | ||
101.82 | 99.91 | 100.65 | 101.45 | ||
X′ ± S.D | 99.88 ± 1.76 | 98.98 ± 1.00 | X′ ± S.D | 100.45 ± 0.36 | 99.85 ± 1.60 |
% RSD | 1.76 | 1.01 | % RSD | 0.36 | 1.60 |
% Error | 1.02 | 0.59 | % Error | 0.21 | 0.92 |
6 | 98.39 | 98.00 | 0.6 | 98.93 | 98.23 |
98.11 | 97.88 | 99.03 | 98.50 | ||
98.51 | 98.26 | 99.57 | 99.03 | ||
X′ ± S.D | 98.34 ± 0.21 | 98.05 ± 0.19 | X′ ± S.D | 99.18 ± 0.34 | 98.58 ± 0.41 |
% RSD | 0.21 | 0.20 | % RSD | 0.35 | 0.41 |
% Error | 0.12 | 0.11 | % Error | 0.20 | 0.24 |
8 | 100.12 | 99.73 | 0.8 | 99.93 | 100.61 |
99.93 | 99.93 | 99.66 | 100.7 | ||
99.54 | 100.88 | 101.01 | 101.15 | ||
X′ ± S.D | 99.86 ± 0.30 | 100.18 ± 0.61 | X′ ± S.D | 100.20 ± 0.71 | 100.82 ± 0.29 |
% RSD | 0.30 | 0.61 | % RSD | 0.71 | 0.29 |
% Error | 0.17 | 0.35 | % Error | 0.41 | 0.17 |