Table 6 Change in the flow rate results (1.1–1.3 mL/min).

From: Rapidly, sensitive quantitative assessment of thiopental via forced stability indicating validated RP-HPLC method and its in-use stability activities

Standard replicate

Flow (1.2 mL)

Flow (1.3 mL)

Flow (1.1 mL)

Weight (mg)

54.2

54.2

54.2

1

5931.4

5510.0

6536.2

2

5944.4

5502.7

6515.0

3

5943.1

5498.4

6525.3

4

5925.0

5518.2

6544.8

5

5940.2

5512.4

6511.7

6

5915.2

5508.7

6582.4

Mean P.A

5933.2

5508.4

6535.9

Tests

 Weight (mg)

54.3

54.1

54.1

  1

5931.1

5523.2

6511.8

  2

5991.3

5538.2

6503.8

 Mean P.A

5961.2

5530.7

6507.8

 Assay (%)

86.0

86.3

85.5

Pooled assay (%)

85.9

Pooled STDEV

0.36

Pooled RSD (%)

0.42