Table 2 NMR spectroscopic data of 6β-hydroxyipolamiide18.
Position | δH | δc | HMBC |
---|---|---|---|
1 | 5.62 (1H, s) | 93.2 | 3, 1’ |
3 | 7.31 (1H, s) | 151.1 | 1, 4, 11 |
4 | – | 114.7 | – |
5 | – | 70.5 | – |
6 | 3.29 (1H, t) | 73.4 | – |
7 | 2.02 (2H, m) | 40.3 | – |
8 | – | 77.8 | – |
9 | 2.26 (1H, s) | 61,2 | 1, 10, 5 |
10 | 0.96 (3H, s) | 23.8 | 9 |
11 | – | 166.3 | – |
12 | 3.60 (3H, s) | 51.3 | 11 |
1’ | 4.36 (1H, d) | 98.4 | 1 |
2’ | 2.91 (1H, m) | 73.4 | 1’ |
3’ | 3.11 (1H, m) | 76.5 | – |
4’ | 3.04 (1H, m) | 70.2 | – |
5’ | 3.02 (1H, m) | 77.3 | – |
6’ | 3.65 (2H, m) | 61.5 | – |