Table 3 Performance assessment of the equipment using three refluxing set-ups.

From: A recirculating device of cooling water powered by solar energy for the laboratory

Solvents

Water

Ethanol

DCM

DCM

Ethanol

Water

Linking order

1

2

3

1

2

3

Boiling point (°C)

100.0

78.3

40.0

40.0

78.3

100.0

Heating temp.(°C)

126

92

80

80

92

126

Reflux time (h)

10

10

10

10

10

10

Solvent loss 1,a

3%

5%

6%

5%

4%

4%

Solvent loss 1,b

0

0

0

0

0

0

  1. 1 working voltage of pump and electric fan is 9 V; a the condenser is open in the air; b the condenser is equipped with an oil bubbler. Temp. Differ. are calculated using the temperature of water in the bucket (Twater) minus the room temperature (Tr.t.). Solvent loss(%) = (Vstart – Vremain)/Vstart × 100%.