Table 1 Conditions of experimental and microstructure characteristics of equiatomic AlCoFeNiTi, AlCoFeNiTiMo HEA alloy samples reported in the literature.

From: Microstructure evolution and catalytic activity of AlCo1−xFeNiTiMox high entropy alloys fabricated by powder metallurgy route

Sample

Equipment

Ball to powder ratio

PCA

Milling time and speed

Structure of powder

Structure of bulk sample

Refs.

AlCoFeNiTi

Planetary ball mill

10:1

45 h dry milling + 4 h ethanol

45 h at 300 rpm

main BCC+ a few FCC

Spark plasma sintering a primary FCC + a BCC + a trace amount of Al3Ti

27

AlCoFeNiTi

Fritsch P-5

10:1

Toluene

300 rpm

BCC

SPS: BCC + TiC

28

AlCoFeNiTi

Fritsch P-5

10:1

Toluene

8 h 300 rpm

BCC

SPS: two BCC (2.95 Å) + BCC(B2 2.916 Å) + TiC

29

AlCoFeNiTi

SPEX 8000 M

10:1

Methanol

15 h

BCC

conventional sintering: BCC (2.87 Å ) + FCC1(3.60 Å) + FCC2(4.27 Å)

30

AlCoFeNiTi

 

25:1

Toluene

30 h 400 rpm

main FCC (3.571 Å) + a few BCC (2.858 Å) + Ni4Ti3

-

31

AlCoFeNiTi

Arc furnace + water-cooled copper mould

-

ingot: L21(Fe2AlTi) + BCC1(Fe, Co, Ni)+ BCC2(Fe, Al Ti) plate: L21 + BCC2

32

AlCoFeNiTiMo

SPEX 8000 M

10:1

methanol

15 h

BCC1 Mo-type + BCC2 Fe-type + FCC

FCC1(3.60 Å) + FCC2 + Co7Mo6

30

AlCoFeNiTiMo

SPEX 8000 M

5:1

methanol

20 h

BCC1 Mo-type BCC2 Fe-type

conventional sintering: FCC + BCC Fe-type, +µCoMo-type + α CoMo-type arc melted ingot: BCC Mo-type, Ti2O

33