Table 1 Comparison of chemical compositions of obtained samples after hydrothermal synthesis.
Tsynthesis (°C) | Starting material | Zr, at. % | O, at. % | Na, at. % | Cl, at. % | N, at. % |
|---|---|---|---|---|---|---|
110 | ZrOCl2·8H2O | 24.9 | 65.7 | 5.5 | 3.9 | – |
ZrO(NO3)2·2H2O | 26.4 | 64.1 | 5.4 | – | 5.1 | |
120 | ZrOCl2·8H2O | 29.7 | 59.9 | 5.8 | 4.6 | – |
ZrO(NO3)2·2H2O | 29.6 | 61.8 | 4.1 | – | 4.5 | |
130 | ZrOCl2·8H2O | 28.2 | 62.8 | 5.2 | 3.8 | – |
ZrO(NO3)2·2H2O | 29.2 | 60.3 | 4.7 | – | 5.8 | |
140 | ZrOCl2·8H2O | 28.6 | 61.5 | 4.4 | 5.5 | – |
ZrO(NO3)2·2H2O | 27.8 | 62.0 | 4.8 | – | 5.4 | |
150 | ZrOCl2·8H2O | 26.6 | 63.7 | 6.5 | 3.2 | – |
ZrO(NO3)2·2H2O | 30.4 | 61.3 | 4.5 | – | 3.8 | |
160 | ZrOCl2·8H2O | 29.6 | 61.7 | 4.4 | 4.3 | – |
ZrO(NO3)2·2H2O | 30.9 | 60.2 | 5.2 | – | 3.7 |
