Table 3 Pulse parameters for \({^1\hbox {H}}-{^{13}\hbox {C}}\) HSQC. Also see Fig. 8.
From: Split spiral broadband double channel NMR detector facilitated by LTCC technology
Parameters | 5/10 spiral | 6/14 spiral |
|---|---|---|
\({^1\hbox {H}}\) RF power (watt) | 10 | 10 |
\({^1\hbox {H}}\)\(\ {90}^{\circ }\) pulse length (µs) | 11 | 11 |
Number of data points in FID | 4096 | 4096 |
\({^13\hbox {C}}\) RF power (watt) | 25 | 30 |
\({^13\hbox {C}}\)\(\ {90}^{\circ }\) pulse length (µs) | 30 | 28 |
Number of data points in FID | 512 | 512 |
Decoupling power (watt) | 0.7 | 0.7 |
Decoupling length (µs) | 20 | 20 |
Number of scans | 8 | 8 |
J-coupling constant J (Hz) | 145 | 145 |
\(\tau =(4J)^{-1}\) (ms) | 1.72 | 1.72 |
Increment delay \(D_0\) (µs) | 3 | 3 |
