Table 2 Refined anomalous dispersion parameters fS′ and fS″ (unit e) for the YLID sulfur atom, compared to tabulated values for the isolated S atom.
Dataset | Refined fS′ | Refined fS″ | Temperature | Crystal |
|---|---|---|---|---|
2 | 0.2694 | 0.6731 | 100 K | Natural shape 1 |
10 | 0.2587 | 0.6214 | 150 K | Natural shape 1 |
15 | 0.3189 | 0.5710 | 292 K | Test crystal 2 |
18 | 0.2865 | 0.5602 | 292 K | Natural shape 2 |
19 | 0.2196 | 0.5625 | 292 K | Test crystal 1 |
20 | 0.2667 | 0.5509 | 292 K | Natural shape 3 |
21 | 0.3681 | 0.5733 | 292 K | Test crystal 3 |
22 | 0.2861 | 0.5629 | 292 K | Test crystal 4 |
23 | 0.1930 | 0.5671 | 292 K | Test crystal 5 |
Average | 0.27(5) | 0.58(4) | – | – |
Cromer & Liberman52 | 0.3331 | 0.5567 | – | – |
Henke et al.54 | 0.3354 | 0.5514 | – | – |
Sasaki55 | 0.328 | 0.590 | – | – |
Brennan & Cowan56 | 0.3338 | 0.5584 | – | – |
