Table 1 Acquisition parameters for triple-resonance NMR experiments
Experiment | HNCO | HNCA | HN(CO)CA | HNCACB | HN(CO)CACB | HN(CA)CB |
|---|---|---|---|---|---|---|
No. of scans | 24 | 64 | 64 | 64 | 56 | 48 |
No. of data points | ||||||
F3 (1H) | 2048 | 2048 | 2048 | 2048 | 2048 | 2048 |
F1 (13C) | 42 | 64 | 128 | 128 | 128 | 128 |
F2 (15N) | 128 | 42 | 42 | 42 | 42 | 42 |