Table 2 Data collection and refinement statistics (molecular replacement).

From: Structure of phospholipase Cε reveals an integrated RA1 domain and previously unidentified regulatory elements

 

PLCε EF3-RA1a

Data collection

 

 Space group

P21

 Cell dimensions

 

  a, b, c (Å)

93.6, 127.8, 139.3

  α, β, γ (°)

90.0 101.1, 90.0

 Resolution (Å)

136.7–2.73 (2.88–2.73)b

 Rmerge

0.268 (0.327)

 I /σI

5.1 (1.1)

 Completeness (%)

99.6 (99.7)

 Redundancy

3.4 (3.5)

Refinement

 

 Resolution (Å)

29.9–2.73

 No. of reflections

80,469

 Rwork / Rfree

0.234/0.273 (0.327/0.381)

 No. of atoms

19,693

  Protein

19,622

  Ligand/ion

4

  Water

67

 B-factors

58.3

  Protein

63.5

  Ligand/ion

109

  Water

38.7

R.m.s. deviations

 

 Bond lengths (Å)

0.011

 Bond angles (°)

1.7

  1. aData was collected from one crystal at GM/CA 23-ID-D.
  2. bValues in parentheses are for highest-resolution shell.
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