Fig. 3: Standard experimental conditions for reproducibility testing. | Communications Chemistry

Fig. 3: Standard experimental conditions for reproducibility testing.

From: Data-science driven autonomous process optimization

Fig. 3

Conditions: 10 µmol 1-E, 1 µmol 1,3,5-trimethoxybenzene, 15 µmol (3-(benzyloxy)phenyl)boronic acid 3, 0.3 µmol Pd(ACN)2Cl2, 0.4 µmol L2, 30 µmol K3PO4 (0.5 M aq) in ACN (0.05 M), 2 h at 20 °C. Average yields for first set of replicates: 2-E: 30(±2)%; 2-Z: 19(±1)% and second set of replicates: 2-E: 28(±2)%; 2-Z: 17(±1)%. Tabulated results are provided in Supplementary Information Table SI-13.

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