Table 1 Electropolymerization of Py monomers under different conditions.
From: Electropolymerization without an electric power supply
Entry | Deviation from optimal conditions | ΔP [MPa]a | Current [μA] | Charge passed [mC]b | Polymer deposition |
---|---|---|---|---|---|
1 | – | 11.6 | 0.21 | 1.40 | Upstream |
2 | Lower flow rate (0.25 mL/min) | 7.3 | 0.10 | 1.37 | Upstream |
3 | Without electrolyte | 10.9 | 0.11 | 0.74 | – |
4 | Without connection between electrodes | 13.4 | – | – | – |
5 | Without Py | 10.1 | 0.21 | 1.36 | – |
6 | Without cotton filling | 0.0 | 0.00 | 0.00 | – |