Table 1 Data collection and refinement statistics
From: Structure of human dipeptidyl peptidase 10 (DPPY): a modulator of neuronal Kv4 channels
hDPP10 | |
|---|---|
Data collection | |
Beamline | APS 19-ID |
Wavelength (Å) | 0.97943 |
Unit cell | A = 80.9 Å b = 143.7 Å c = 176.2 Å |
Space group | P212121 |
Resolution range (Å)* | 66.5–3.4 (3.58–3.40) |
Completeness (%) | 99.9 (99.9) |
Multiplicity | 5.1 (5.0) |
Rsym | 0.226 (0.775) |
Rpim | 0.11 (0.378) |
<I/σI> | 6.8 (2.3) |
Unique reflections | 29019 |
Refinement | |
R/Rfree | 0.207/0.241 |
r.m.s.-deviations | |
bond length (Å) | 0.008 |
bond angle (°) | 1.36 |
Estimate coordinate error (Å) | 0.37 |
Number of atoms | |
protein | 11600 |
carbohydrate | 229 |
B-factors (Å2) | |
protein | 75.7 |
carbohydrate | 107.5 |
