Table 1 Data collection and refinement statistics

Wavelength (Å)

1.0000

Resolution (Å)^a

50.0–3.35 (3.41–3.35)

Space group

P2₁2₁2₁

Cell dimensions

 a, b, c (Å)

87.2, 91.3, 123.4

 α, β, γ (°)

90, 90, 90

No. of unique reflections

14,509

Completeness (%)^a

99.2 (97.2)

R_sym (%)^a,b

13.0 (40.7)

I/σΙ^a

14.3 (1.9)

Redundancy^a

9.5 (5.9)

Refinement

No. of atoms

 Protein

4891

 NAG

56

R_work/R_free (%)^c

23.46/28.65

R.m.s.d.

 Bond lengths (Å)

0.005

 Bond angles (°)

1.113

Average B-factor

 Protein

109.6

 NAG

111.2

Ramachandran plot

 Most favored (%)

83.6

 Disallowed (%)

0.0