Table 3 13C NMR spectroscopic data (chemical shifts [ppm]) of isolated compounds (500 MHz, DMSO-d6).
Position | Compounds | |||||
|---|---|---|---|---|---|---|
1 | 2 | 3 | 4 | 5 | 6 | |
1 | 126.44 | |||||
2 | 73.51 | 153.60 | 130.43 | 147.28 | 147.29 | 154.15 |
3 | 36.08 | 123.63 | 115.54 | 136.14 | 136.10 | 123.84 |
4 | 33.84 | 175.08 | 160.22 | 176.27 | 176.35 | 175.15 |
5 | 133.75 | 127.76 | 115.54 | 161.13 | 161.15 | 127.44 |
6 | 111.59 | 115.67 | 130.43 | 98.65 | 98.67 | 116.11 |
7 | 160.09 | 163.05 | 164.30 | 164.35 | 161.91 | |
8 | 106.89 | 102.59 | 93.85 | 93.96 | 103.86 | |
9 | 158.92 | 157.92 | 156.60 | 156.64 | 157.52 | |
10 | 117.35 | 117.08 | 103.45 | 103.49 | 118.91 | |
1′ | 124.98 | 124.71 | 113.15 | 120.51 | 122.12 | 124.47 |
2′ | 152.08 | 130.54 | 165.54 | 148.13 | 129.97 | 130.57 |
3′ | 140.06 | 114.08 | 102.50 | 145.49 | 115.91 | 114.10 |
4′ | 155.66 | 159.43 | 166.18 | 115.47 | 159.63 | 159.49 |
3′O-CH3 | 63.61 | |||||
4′O-CH3 | 58.78 | 55.62 | 55.62 | |||
5′ | 125.36 | 114.08 | 107.99 | 116.05 | 115.91 | 114.10 |
6′ | 106.36 | 130.54 | 131.97 | 122.40 | 129.97 | 130.57 |
1″ | 100.42 | |||||
2″ | 73.59 | |||||
3″ | 76.93 | |||||
4″ | 70.07 | |||||
5″ | 77.67 | |||||
6″ | 61.09 | |||||
α | 116.95 | |||||
β | 144.16 | |||||
CO | 192.01 | |||||