Table 1 Tempering conditions and the lattice parameters, crystalline size, electrical properties of FTO films.

From: Reference of Temperature and Time during tempering process for non-stoichiometric FTO films

Tempered conditions

volume of unit cell V (Å3)

Crystalline size D (nm)

Hall coefficient Rh(×10−2 cm3·C−1)

mean free path l(nm)

l/D

calculated emissivity ε

Temperature

Time

600 °C

 

72.596

20.08

−1.23

3.80

18.92%

0.24

650 °C

 

72.918

20.26

−1.41

3.73

18.41%

0.27

680 °C

220 s

73.002

21.60

−1.85

4.04

18.70%

0.34

700 °C

 

72.625

21.10

−1.65

3.22

15.26%

0.36

720 °C

 

72.890

19.65

−1.72

1.60

8.14%

0.54

 

150 s

72.509

20.99

−1.51

3.22

15.34%

0.27

 

190 s

72.652

21.30

−1.45

3.80

17.84%

0.32

700 °C

220 s

72.625

21.10

−1.65

3.22

15.26%

0.36

 

260 s

72.688

21.49

−1.87

2.94

13.68%

0.38

 

300 s

72.771

21.11

−2.90

0.97

4.59%

0.45